Article View: sci.materials
Article #212Re: High Vacuum Epoxy
From: William E. Johns;S23015
Date: Fri, 21 Aug 1992 01:12
Date: Fri, 21 Aug 1992 01:12
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2330 bytes
In article <1992Aug20.154626.20676@dirac.physics.sunysb.edu> danube@dirac.physics.sunysb.edu (Dan Koller*) writes:
>
> Does anybody know the absolute ultimate lowest obtainable outgass
>rate of Varian's "Torr-Seal" high vacuum epoxy? Varian Spec. sheets
>only list confusing figures, after short 130 degree bakeouts. I would
>like to know if baking out for a week or so at 130 deg. C will help
>bring the outgass rate below 10e-8 Torr-liter/cm^2/second.
> I would like to use the epoxy to seal sapphire windows to a small
>(1 cm^3) glass chamber, pump it down to better than 10e-7 torr, and then
>seal it off. The problem is that the epoxy seems to be outgassing at
>a rate high enough to bring the pressure to 1 mTorr in a minute or so.
>This is to be expected from Varian's published outgass rates, but my
>question is, can I do better?
> Finally, if epoxy won't work, is there a better way of attaching
>sapphire or Silicon windows to glass?
> Thanks in advance.
> Danube
It has been awhile since I worked on a vacuum bench, but I am
reasonably sure that someone makes a special wax that can be
used for gluing things together. This wax was designed for
high vacuum work. I have no idea where you can get it.
Ride Free,
Bill
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Newsgroups: sci.materials Path: arc1-ca.pugleaf.net!sparky!uunet!haven.umd.edu!darwin.sura.net!mips!sdd.hp.com!usc!sol.ctr.columbia.edu!destroyer!ubc-cs!uw-beaver!news.u.washington.edu!serval!wsuaix.csc.wsu.edu!bill From: bill@wsuaix.csc.wsu.edu (William E. Johns;S23015) Subject: Re: High Vacuum Epoxy Message-ID: <1992Aug21.011236.19058@serval.net.wsu.edu> Sender: Bill Johns Organization: Washington State University References: <1992Aug20.154626.20676@dirac.physics.sunysb.edu> Date: Fri, 21 Aug 92 01:12:36 GMT Lines: 36