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Article #314

identifying polymer cross linking

#314
From: Dwight D. Brantley
Date: Tue, 15 Dec 1992 22:41
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I have been experimenting with determining the integrity of cross linked
polymers.  So far I have exposing my samples in an oxygen rich plasma etch
for 10 minutes then analyzing the sample in a SEM.  I think we are seeing
that examples of proper or "good" cross linked polymers show a grain of
structure of uniform size and orientation while the "bad" samples seem
to display a wide variation of grain size over a given area.  Is this a
viable method of analyzing such materials?  Can anyone add anything to
this?  I am not very familiar with such materials so consider me mostly
ignorant on this subject.  Any information (in simple terms) would be of
great help.

Thanks,

      ******************************************************************
      *   Dwight Brantley    *   Failure Analysis & Reliability Dept.  *
      *  Intergraph, Corp.   *  Reply To: brantley@falab1.b21.ingr.com *
      *   Huntsville, AL     *           Voice: 205-730-4456           *
      ******************************************************************
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Message-ID: <1992Dec15.224100.25463@infonode.ingr.com>
Path: arc1-ca.pugleaf.net!sparky!uunet!infonode!brantley

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Newsgroups: sci.materials
Path: arc1-ca.pugleaf.net!sparky!uunet!infonode!brantley
From: brantley@infonode.ingr.com (Dwight D. Brantley)
Subject: identifying polymer cross linking
Message-ID: <1992Dec15.224100.25463@infonode.ingr.com>
Organization: Intergraph Corporation, Huntsville, AL.
Distribution: usa
Date: Tue, 15 Dec 1992 22:41:00 GMT
Lines: 19