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Article #408

Cleaning Calcium chips

#408
From: danube
Date: Fri, 08 Jan 1993 22:35
11 lines
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    I have some chips of Calcium that are badly oxidized.  I am wondering
if there is a simple way to clean them.  I put them in a plastic bottle
with N2 gas and sealed it for storage.  I noticed that if I shake the 
bottle a lot, the oxide rubs off a bit.  I suppose I could put glass chips
in the bottle and shake for a day.  Then I could take the Ca chips out in
a glove box.
    Any better Ideas?  Also, how can I store things like Ca, Na, K, and Rb
without oil?  Is Carbon-tetrachloride better?  I need to put the chips in
a high vacuum system and I don't want the oil around.  I assume things like
C-tet evaporate more easily.
							Danube
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Newsgroups: sci.materials
Path: arc1-ca.pugleaf.net!sparky!uunet!wupost!udel!sbcs.sunysb.edu!insti!danube
From: danube@max.physics.sunysb.edu
Subject: Cleaning Calcium chips
Message-ID: <C0K42H.C75@max.physics.sunysb.edu>
Organization: Institute for the Theoretical Physics
Date: Fri, 8 Jan 1993 22:35:05 GMT
Lines: 11