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Article #408Cleaning Calcium chips
From: danube
Date: Fri, 08 Jan 1993 22:35
Date: Fri, 08 Jan 1993 22:35
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I have some chips of Calcium that are badly oxidized. I am wondering
if there is a simple way to clean them. I put them in a plastic bottle
with N2 gas and sealed it for storage. I noticed that if I shake the
bottle a lot, the oxide rubs off a bit. I suppose I could put glass chips
in the bottle and shake for a day. Then I could take the Ca chips out in
a glove box.
Any better Ideas? Also, how can I store things like Ca, Na, K, and Rb
without oil? Is Carbon-tetrachloride better? I need to put the chips in
a high vacuum system and I don't want the oil around. I assume things like
C-tet evaporate more easily.
Danube
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Newsgroups: sci.materials Path: arc1-ca.pugleaf.net!sparky!uunet!wupost!udel!sbcs.sunysb.edu!insti!danube From: danube@max.physics.sunysb.edu Subject: Cleaning Calcium chips Message-ID: <C0K42H.C75@max.physics.sunysb.edu> Organization: Institute for the Theoretical Physics Date: Fri, 8 Jan 1993 22:35:05 GMT Lines: 11